Field emission scanning electron microscope(FE-SEM)
Field Emission Scanning Electron Microscope
Operating
Model: ULTRA PLUS
Function: High-resolution microscopic morphology observation and micro-area compositional analysis.
Engineer: Teacher Wang / +86-21- 34207734-8006 / wangying@1
Location: West Area,Testing Zone II
Equipment ID: WT2ZSEM01
  • Basic Equipment Information
  • Operating Principle
  • Typical Application Case
Main Application

It is primarily used for ultra-high-resolution microscopic morphology observation of micro- and nano-scale materials and structures. It can also be combined with an energy-dispersive X-ray spectroscopy (EDS) system to perform micro-area compositional analysis of material or structure surfaces and cross-sections.

 

Process/Testing Capabilities

Field emission scanning electron microscopy (FE-SEM) is widely used in the inspection of semiconductors, inorganic non-metallic materials, and devices due to its high resolution, large depth of field, enhanced stereoscopic imaging, and wide adjustable magnification range.

It enables secondary electron imaging and backscattered electron imaging of surface morphology for various solid samples, as well as image processing. When equipped with an energy-dispersive X-ray spectroscopy (EDS) system, it can perform qualitative, semi-quantitative, and quantitative elemental analysis at micro-regions (point, line, and area) on the sample surface. It provides integrated analytical capabilities for both morphology and chemical composition.

 

Technical Specifications

1. Resolution: ≤ 0.8 nm @ 15 V; ≤ 1.6 nm @ 1 kV

2. Accelerating voltage: 0.02 kV–30 kV; excellent low-voltage performance suitable for observing low-conductivity samples

3. Detectors: in-lens high-efficiency secondary electron detector and energy-selective backscattered electron detector; chamber-mounted high-efficiency secondary electron detector and angle-selective backscattered electron detector, enabling simultaneous acquisition of SE and BSE images

4. Sample stage: maximum sample size Φ200 mm

5. Five-axis motorized eucentric stage, tilt range -3° to 70°, continuous 360° rotation

6. Equipped with EDS system for micro-area compositional analysis

7. Ion sputter coater for gold (Au) coating deposition

Field emission scanning electron microscopy (FE-SEM) uses a field emission electron source to generate a high-energy electron beam, which is focused onto the sample surface through an electromagnetic lens system. When the electron beam interacts with the sample, signals such as backscattered electrons, scattered electrons, and secondary electrons are generated. These signals are collected and converted into images, enabling observation and analysis of the sample’s surface microstructure.

When equipped with an energy-dispersive X-ray spectroscopy (EDS) system, it allows simultaneous microscopic morphology observation and micro-area compositional analysis.

Scanning electron microscopy (SEM) image.

EDS analysis

 

[Please arrive at the laboratory at least 15 minutes in advance to prepare the sample]Magnetic and powder samples are not allowed. Samples must be kept clean, and direct contact with hands is prohibited. The maximum wafer size is 6 inches.
Sample requirements:

1.The sample must be a dry, anhydrous solid with no volatile solvents.

2.Non-magnetic materials only.

3.Porous materials must be pre-vacuumed prior to operation.Self-service operating hours:11:30–13:30 (noon) and 17:00–22:00 daily.

The list below shows FAQs (click a question to view the answer). If your question is not listed, you can leave a message using the link.
FAQs
  • 01
    EDS有哪些测试模式?

    EDS有点测、线扫描、面扫描模式。

    A. 点测是在样品上选择一个微小的区域进行分析测量,获得包括元素种类及相对含量等信息。

    B. 线扫是沿着一条线进行连续测量,得到这条线上成分变化情况。

    C. 面扫是在样品表面选择一个面进行扫描,获取整个区域的元素分布信息。

  • 02
    SEM拍样品截面如何制样?

    A. 对于硅片、玻璃片等可采用划片进行切割,露出需要观测的位置;

    B. 样品垂直贴于样品台上,观测面朝上。

  • 03
    SEM样品制备一般有什么要求?

    A. 要确保分析的位置被暴露出来;

    B. 样品表面导电性良好,如导电性不好可采用喷金或喷碳增加导电性;

    C.样品无易挥发物质;

    D.不易被电子束损伤。

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